Analysis of odorous gases with simultaneous GC-MS and sensory determination

Inka Orko, Jukka Lehtomäki, Erik Sandell, Mona Arnold

    Research output: Book/ReportReport

    Abstract

    Industrial odorous off-gases can consist of hundreds of different compounds giving cause to odour annoyance in the vicinity of the odour-emitting plant. For the identification of the odorous components in the gas, traditional analytical methods are not always sufficient since the odour threshold values cannot often be found in literature. This report decribes the development of a GC-MS sniffing port method for identifying odorous compounds in off-gases. In the method the sample is injected into a gas chromatograph and divided into two flows. The compounds in these sample flows are separated in two identical columns and detected simultaneously in a mass spectrometer and by sensory means. The olfactory detections are marked in the iongram and the odorous compounds are identified. Tenax TA adsorbent is generally used for collecting the odorous sample for analysis. The compounds are released from the adsorbent for analysis by thermal desorption. The report also decribes a case study where the GC-MS sniffing port method was applied to a gaseous emission from a food factory. Over ten odorous compounds could be identified.
    Original languageEnglish
    Place of PublicationEspoo
    PublisherVTT Technical Research Centre of Finland
    Number of pages26
    ISBN (Print)951-38-4864-7
    Publication statusPublished - 1995
    MoE publication typeNot Eligible

    Publication series

    SeriesVTT Tiedotteita - Meddelanden - Research Notes
    Number1710
    ISSN1235-0605

    Keywords

    • analyzing
    • odors
    • gases
    • industrial plants
    • emissions
    • off-gases
    • odor control
    • odor detections
    • odor emissions
    • methods
    • detectors
    • measuring instruments

    Fingerprint Dive into the research topics of 'Analysis of odorous gases with simultaneous GC-MS and sensory determination'. Together they form a unique fingerprint.

    Cite this