Determination of toxic PCB congeners in biological samples by multidimensional gas chromatography-mass spectrometry (GC/GC/MS)

Erkki Sippola; Kimmo Himberg

doi:10.1007/BF00323809

Determination of toxic PCB congeners in biological samples by multidimensional gas chromatography-mass spectrometry (GC/GC/MS)

Erkki Sippola^*
, Kimmo Himberg

^*Corresponding author for this work

VTT Technical Research Centre of Finland

VTT (former employee or external)

Research output: Contribution to journal › Article › Scientific › peer-review

27 Citations (Scopus)

Abstract

Multidimensional gas chromatography-mass spectrometry (GC/GC/MS) was used for the determination of coplanar PCB congeners in biological samples. A quadrupole low resolution mass spectrometer was used as the main detector in order to increase the reliability of identification and enable the use of ¹³C-labelled internal standards. The technique was capable to separate these toxic congeners from the complex matrix and decreased the need of sample purification.

Original language	English
Pages (from-to)	510-512
Journal	Fresenius' Journal of Analytical Chemistry
Volume	339
Issue number	7
DOIs	https://doi.org/10.1007/BF00323809
Publication status	Published - 1991
MoE publication type	A1 Journal article-refereed

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10.1007/BF00323809

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title = "Determination of toxic PCB congeners in biological samples by multidimensional gas chromatography-mass spectrometry (GC/GC/MS)",

abstract = "Multidimensional gas chromatography-mass spectrometry (GC/GC/MS) was used for the determination of coplanar PCB congeners in biological samples. A quadrupole low resolution mass spectrometer was used as the main detector in order to increase the reliability of identification and enable the use of 13C-labelled internal standards. The technique was capable to separate these toxic congeners from the complex matrix and decreased the need of sample purification.",

author = "Erkki Sippola and Kimmo Himberg",

note = "Project code: ELI04010",

year = "1991",

doi = "10.1007/BF00323809",

language = "English",

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journal = "Fresenius' Journal of Analytical Chemistry",

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T1 - Determination of toxic PCB congeners in biological samples by multidimensional gas chromatography-mass spectrometry (GC/GC/MS)

AU - Sippola, Erkki

AU - Himberg, Kimmo

N1 - Project code: ELI04010

PY - 1991

Y1 - 1991

N2 - Multidimensional gas chromatography-mass spectrometry (GC/GC/MS) was used for the determination of coplanar PCB congeners in biological samples. A quadrupole low resolution mass spectrometer was used as the main detector in order to increase the reliability of identification and enable the use of 13C-labelled internal standards. The technique was capable to separate these toxic congeners from the complex matrix and decreased the need of sample purification.

AB - Multidimensional gas chromatography-mass spectrometry (GC/GC/MS) was used for the determination of coplanar PCB congeners in biological samples. A quadrupole low resolution mass spectrometer was used as the main detector in order to increase the reliability of identification and enable the use of 13C-labelled internal standards. The technique was capable to separate these toxic congeners from the complex matrix and decreased the need of sample purification.

U2 - 10.1007/BF00323809

DO - 10.1007/BF00323809

M3 - Article

SN - 0937-0633

VL - 339

SP - 510

EP - 512

JO - Fresenius' Journal of Analytical Chemistry

JF - Fresenius' Journal of Analytical Chemistry

IS - 7

ER -

Determination of toxic PCB congeners in biological samples by multidimensional gas chromatography-mass spectrometry (GC/GC/MS)

Abstract

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