Differential photoacoustic gas cell based on LTCC for ppm gas sensing

Kimmo Keränen, Kari Kautio, Jyrki Ollila, Mikko Heikkinen, I. Kauppinen, T. Kuusela, B. Matveev, M. E. McNie, R. M. Jenkins, P. Karioja

    Research output: Chapter in Book/Report/Conference proceedingConference article in proceedingsScientificpeer-review

    2 Citations (Scopus)


    Silicon MEMS cantilever-based photoacoustic technology allows for the sensing of ultra low gas concentrations with very wide dynamic range.
    The sensitivity enhancement is achieved with a cantilever microphone system in which the cantilever displacement is probed with an optical interferometer providing a pico-meter resolution. In the gas sensor, the silicon cantilever microphone is placed in a two-chamber differential gas cell.
    By monitoring differential pressure changes between the two chambers, the differential cell operates as a differential infra-red detector for optical absorption signals through a measurement and reference path. The differential pressure signal is proportional to gas concentration in the optical measurement path. We have designed, implemented and tested a differential photo-acoustic gas cell based on Low Temperature Co-fired Ceramic (LTCC) multilayer substrate technology.
    Standard LTCC technology enables implementation of 2.5D structures including holes, cavities and channels into the electronic substrate. The implemented differential photoacoustic gas cell structure includes two 10 mm long cylindrical cells, diameter of 2.4 mm.
    Reflectance measurements of the cell showed that reflectivity of the substrate material can be improved by a factor 15 - 90 in the 3 - 8 μm spectral region using gold or silver paste coatings. A transparent window is required in the differential gas cell structure in order to probe the displacement of the silicon cantilever.
    The transparent sapphire window was sealed to the LTCC substrate using two methods: screen printed Au80/Sn20 solder paste and pre-attached glass solder paste (Diemat DM2700P/H848). Both methods were shown to provide hermetic sealing of sapphire windows to LTCC substrate.
    The measured He-leak rate for the 10 sealed test samples implemented using glass paste were under 2.0 ×10-9 atm×cm3/s, which meets the requirement for the leak rate according to MIL-STD 883. The achieved hermeticity level suggests that the proof-of-principle packaging demonstrator paves the way for implementing a novel differential photoacoustic gas cell for a future miniature gas sensor module.
    The future module consisting of a sample gas cell and immersion lens IR LEDs together with interferometric probing of the cantilever microphone is expected to be capable of measuring ultra low concentrations of a wide range of gases with their fundamental absorption bands at 3 - 7 μm wavelength, such as CO, CO2 and CH4.
    Original languageEnglish
    Title of host publicationProceedings of the SPIE
    Subtitle of host publicationOptoelectronic Interconnects and Component Integration IX
    PublisherInternational Society for Optics and Photonics SPIE
    Number of pages12
    ISBN (Print)978-0-8194-8003-3
    Publication statusPublished - 2010
    MoE publication typeA4 Article in a conference publication
    EventOptoelectronic Interconnects and Component Integration IX - San Francisco, CA, United States
    Duration: 25 Jan 201027 Jan 2010

    Publication series

    SeriesProceedings of SPIE


    ConferenceOptoelectronic Interconnects and Component Integration IX
    Country/TerritoryUnited States
    CitySan Francisco, CA


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