MOVPE growth of N-polar AlN on 4H-SiC: Effect of substrate miscut on layer quality

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Abstract

We present the effect of miscut angle of SiC substrates on N-polar AlN growth. The N-polar AlN layers were grown on C-face 4H-SiC substrates with a miscut towards 〈1¯100〉 by metal-organic vapor phase epitaxy (MOVPE). The optimal V/III ratios for high-quality AlN growth on 1° and 4° miscut substrates were found to be 20,000 and 1000, respectively. MOVPE grown N-polar AlN layer without hexagonal hillocks or step bunching was achieved using a 4H-SiC substrate with an intentional miscut of 1° towards 〈1¯100〉. The 200-nm-thick AlN layer exhibited X-ray rocking curve full width half maximums of 203 arcsec and 389 arcsec for (0 0 2) and (1 0 2) reflections, respectively. The root mean square roughness was 0.4 nm for a 2 μm×2μm atomic force microscope scan.
Original languageEnglish
Pages (from-to)12-16
JournalJournal of Crystal Growth
Volume487
DOIs
Publication statusPublished - 1 Apr 2018
MoE publication typeA1 Journal article-refereed

Funding

This work was supported by the Academy of Finland (grant 297916 ), the Foundation for Aalto University Science and Technology and JSPS KAKENHI Grant No. 16H06424 and 17K14110. The research was performed at the OtaNano - Micronova Nanofabrication Centre of Aalto University.

Keywords

  • A1. Polarity
  • A1. X-ray diffraction
  • A3. Metal-organic vapor phase epitaxy
  • B1. Nitrides
  • B2. Semiconducting aluminum compounds

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