Nickel‐Electrocatalyzed Synthesis of Bifuran‐Based Monomers

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Abstract

Bifuran motifs can be accessed with nickel-bipyridine electrocatalyzed homocouplings of bromine-substituted methyl furancarboxylates, which, in turn, can be prepared from hemicellulose-derived furfural. The described protocol uses sustainable carbon-based graphite electrodes in the simplest setup – an undivided cell with constant current electrolysis. The reported method avoids using a sacrificial anode by employing triethanolamine as an electron donor.
Original languageEnglish
Article numbere202302572
JournalChemistry - A European Journal
Volume29
Issue number71
DOIs
Publication statusPublished - 19 Dec 2023
MoE publication typeA1 Journal article-refereed

Funding

Kiia Malinen from Aalto University is acknowledged for her help preparing this manuscript. T. W. is grateful for financial support from the Research Council of Finland (Grant no. 348889).

Keywords

  • Catalysis
  • Electrochemistry
  • Molecular Electrochemistry

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