Problems of studying the crystal structure of Ce1-xLax11B6 solid solutions by high-resolution powder neutron diffraction

Vitali Trunov, A. Malyshev, D. Chernyshov, A. Kurbakov, M. Korsukova (Corresponding Author), V. Gurin, Olli Antson, Pekka Hiismäki

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    Abstract

    The crystal structure of Ce1 - xLax11B6 solid solutions for various x has been studied by high-resolution powder neutron diffraction. A correction for the effect of primary extinction was applied to integrated intensities in a Rietveld program. The refinement results demonstrate good agreement with the data of X-ray single-crystal diffractometer studies performed on the same samples. Vacancies at the boron site and complete occupancy of the metal position are established for all compositions studied. The refined values of the Ce/La ratio at the metal site are in good agreement with those determined by X-ray fluorescence spectrometry on single crystals.
    Original languageEnglish
    Pages (from-to)142 - 145
    Number of pages4
    JournalJournal of Applied Crystallography
    Volume24
    Issue numberPart 2
    DOIs
    Publication statusPublished - 1991
    MoE publication typeA1 Journal article-refereed

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    Trunov, V., Malyshev, A., Chernyshov, D., Kurbakov, A., Korsukova, M., Gurin, V., Antson, O., & Hiismäki, P. (1991). Problems of studying the crystal structure of Ce1-xLax11B6 solid solutions by high-resolution powder neutron diffraction. Journal of Applied Crystallography, 24(Part 2), 142 - 145. https://doi.org/10.1107/S0021889890011542