Problems of studying the crystal structure of Ce1-xLax11B6 solid solutions by high-resolution powder neutron diffraction

Vitali Trunov, A. Malyshev, D. Chernyshov, A. Kurbakov, M. Korsukova (Corresponding Author), V. Gurin, Olli Antson, Pekka Hiismäki

    Research output: Contribution to journalArticleScientificpeer-review

    5 Citations (Scopus)

    Abstract

    The crystal structure of Ce1 - xLax11B6 solid solutions for various x has been studied by high-resolution powder neutron diffraction. A correction for the effect of primary extinction was applied to integrated intensities in a Rietveld program. The refinement results demonstrate good agreement with the data of X-ray single-crystal diffractometer studies performed on the same samples. Vacancies at the boron site and complete occupancy of the metal position are established for all compositions studied. The refined values of the Ce/La ratio at the metal site are in good agreement with those determined by X-ray fluorescence spectrometry on single crystals.
    Original languageEnglish
    Pages (from-to)142 - 145
    Number of pages4
    JournalJournal of Applied Crystallography
    Volume24
    Issue numberPart 2
    DOIs
    Publication statusPublished - 1991
    MoE publication typeA1 Journal article-refereed

    Fingerprint

    Neutron Diffraction
    Powder Diffraction
    Neutron powder diffraction
    Solid solutions
    Crystal structure
    Metals
    Single crystals
    X-Ray Emission Spectrometry
    Boron
    Diffractometers
    Vacancies
    X-Rays
    X rays
    Chemical analysis

    Cite this

    Trunov, V., Malyshev, A., Chernyshov, D., Kurbakov, A., Korsukova, M., Gurin, V., ... Hiismäki, P. (1991). Problems of studying the crystal structure of Ce1-xLax11B6 solid solutions by high-resolution powder neutron diffraction. Journal of Applied Crystallography, 24(Part 2), 142 - 145. https://doi.org/10.1107/S0021889890011542
    Trunov, Vitali ; Malyshev, A. ; Chernyshov, D. ; Kurbakov, A. ; Korsukova, M. ; Gurin, V. ; Antson, Olli ; Hiismäki, Pekka. / Problems of studying the crystal structure of Ce1-xLax11B6 solid solutions by high-resolution powder neutron diffraction. In: Journal of Applied Crystallography. 1991 ; Vol. 24, No. Part 2. pp. 142 - 145.
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    title = "Problems of studying the crystal structure of Ce1-xLax11B6 solid solutions by high-resolution powder neutron diffraction",
    abstract = "The crystal structure of Ce1 - xLax11B6 solid solutions for various x has been studied by high-resolution powder neutron diffraction. A correction for the effect of primary extinction was applied to integrated intensities in a Rietveld program. The refinement results demonstrate good agreement with the data of X-ray single-crystal diffractometer studies performed on the same samples. Vacancies at the boron site and complete occupancy of the metal position are established for all compositions studied. The refined values of the Ce/La ratio at the metal site are in good agreement with those determined by X-ray fluorescence spectrometry on single crystals.",
    author = "Vitali Trunov and A. Malyshev and D. Chernyshov and A. Kurbakov and M. Korsukova and V. Gurin and Olli Antson and Pekka Hiism{\"a}ki",
    year = "1991",
    doi = "10.1107/S0021889890011542",
    language = "English",
    volume = "24",
    pages = "142 -- 145",
    journal = "Journal of Applied Crystallography",
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    Trunov, V, Malyshev, A, Chernyshov, D, Kurbakov, A, Korsukova, M, Gurin, V, Antson, O & Hiismäki, P 1991, 'Problems of studying the crystal structure of Ce1-xLax11B6 solid solutions by high-resolution powder neutron diffraction', Journal of Applied Crystallography, vol. 24, no. Part 2, pp. 142 - 145. https://doi.org/10.1107/S0021889890011542

    Problems of studying the crystal structure of Ce1-xLax11B6 solid solutions by high-resolution powder neutron diffraction. / Trunov, Vitali; Malyshev, A.; Chernyshov, D.; Kurbakov, A.; Korsukova, M. (Corresponding Author); Gurin, V.; Antson, Olli; Hiismäki, Pekka.

    In: Journal of Applied Crystallography, Vol. 24, No. Part 2, 1991, p. 142 - 145.

    Research output: Contribution to journalArticleScientificpeer-review

    TY - JOUR

    T1 - Problems of studying the crystal structure of Ce1-xLax11B6 solid solutions by high-resolution powder neutron diffraction

    AU - Trunov, Vitali

    AU - Malyshev, A.

    AU - Chernyshov, D.

    AU - Kurbakov, A.

    AU - Korsukova, M.

    AU - Gurin, V.

    AU - Antson, Olli

    AU - Hiismäki, Pekka

    PY - 1991

    Y1 - 1991

    N2 - The crystal structure of Ce1 - xLax11B6 solid solutions for various x has been studied by high-resolution powder neutron diffraction. A correction for the effect of primary extinction was applied to integrated intensities in a Rietveld program. The refinement results demonstrate good agreement with the data of X-ray single-crystal diffractometer studies performed on the same samples. Vacancies at the boron site and complete occupancy of the metal position are established for all compositions studied. The refined values of the Ce/La ratio at the metal site are in good agreement with those determined by X-ray fluorescence spectrometry on single crystals.

    AB - The crystal structure of Ce1 - xLax11B6 solid solutions for various x has been studied by high-resolution powder neutron diffraction. A correction for the effect of primary extinction was applied to integrated intensities in a Rietveld program. The refinement results demonstrate good agreement with the data of X-ray single-crystal diffractometer studies performed on the same samples. Vacancies at the boron site and complete occupancy of the metal position are established for all compositions studied. The refined values of the Ce/La ratio at the metal site are in good agreement with those determined by X-ray fluorescence spectrometry on single crystals.

    U2 - 10.1107/S0021889890011542

    DO - 10.1107/S0021889890011542

    M3 - Article

    VL - 24

    SP - 142

    EP - 145

    JO - Journal of Applied Crystallography

    JF - Journal of Applied Crystallography

    SN - 0021-8898

    IS - Part 2

    ER -