Surface modification of He pre-exposed tungsten samples by He plasma impact in the divertor manipulator of ASDEX Upgrade

S. Brezinsek, A. Hakola, H. Greuner, M. Balden, A. Kallenbach, M. Oberkofler, G. De Temmerman, D. Douai, A. Lahtinen, B. Böswirth, D. Brida, R. Caniello, D. Carralero, S. Elgeti, K. Krieger, H. Mayer, G. Meisl, S. Potzel, V. Rohde, B. SieglinA. Terra, R. Neu, Ch. Linsmeier, EUROfusion MST1 Team

    Research output: Contribution to journalArticleScientificpeer-review

    7 Citations (Scopus)

    Abstract

    Tungsten (W) will be used as material for plasma-facing components (PFCs) in the divertor of ITER and interact with Helium (He) ions either from initial He plasma operation or from Deuterium-Tritium (DT) fusion reactions in the active operation phase. Laboratory experiments reported that in a specific operational window of impact energy, ion fluence, and surface temperature (E in ≥ 20 eV, ϕ ≥ 1 × 10 24 He+mB t=2.5T,I p=0.8MA,P aux≃8.0MW T surf ≥ 1000 K) a modification of W surfaces occurs resulting in the formation of He-induced W nanostructures. Experiments in ASDEX Upgrade H-mode plasmas (E in=37keV T, ϕ≃0.75×10 24He 0m −2 MA, P aux ≃ 8.0 MW) in He have been carried out to investigate in detail (a) the potential growth of W nanostructures on pre-damaged W samples incorporating He nanobubbles, and (b) the potential ELM-induced erosion of W nanostructure. Both W surface modifications were generated artificially in the GLADIS facility by He bombardment of W samples at ϕ≃1×10 24He 0m −2 keV (a) to ϕ ≃ 0.75 × 10 24 He 0mϕ≃1.6×10 24He +m −2 at T surf ≃ 1800 K and (b) ϕ ≃ 1 × 10 24 He 0m−2 at T surf ≃ 2300 K prior to exposure in the divertor manipulator of ASDEX Upgrade. Though in part (a) conditions of W nanostructure growth with a total He ion fluence of ϕ ≃ 1.6 × 10 24 He+m−2 and peak He ion impact energies above 150 eV were met, no growth could be detected. In part (b) lower density plasmas with more pronounced type I ELMs, carrying energetic He ions in the keV range, were executed with the strike-line positioned on 2 µm thick W nanostructure accumulating a fluence of ϕ ≃ 0.8 × 10 24 He+m−2. Post-mortem analysis revealed that co-deposition by predominantly W, and Boron (B), eroded at the main chamber wall and transported into the divertor, took place on all W samples. Erosion of W nanostructure or its formation was hindered by the fact that the outer divertor at the location of the samples was turned under these He plasma conditions into a net deposition zone by W, B and Carbon (C) ions. The surface morphology with large roughness and effective surface area act as a catcher for the impinging impurities. Thus, apart from operation in the existence diagram of W nanostructure with respect to T surf, ϕ, and E in, also the impinging impurity flux contribution needs to be considered in predictions concerning the formation of W nanostructures.

    Original languageEnglish
    Pages (from-to)575-581
    Number of pages7
    JournalNuclear Materials and Energy
    Volume12
    DOIs
    Publication statusPublished - 1 Aug 2017
    MoE publication typeA1 Journal article-refereed

    Fingerprint

    helium plasma
    Helium
    Tungsten
    Manipulators
    Surface treatment
    manipulators
    tungsten
    helium
    Plasmas
    helium ions
    Nanostructures
    Ions
    fluence
    erosion
    nanostructure growth
    catchers
    impurities
    ion impact
    tritium
    Erosion

    Keywords

    • PSI
    • ASDEX Upgrade
    • ITER
    • W divertor
    • W nanostructure
    • helium

    Cite this

    Brezinsek, S. ; Hakola, A. ; Greuner, H. ; Balden, M. ; Kallenbach, A. ; Oberkofler, M. ; De Temmerman, G. ; Douai, D. ; Lahtinen, A. ; Böswirth, B. ; Brida, D. ; Caniello, R. ; Carralero, D. ; Elgeti, S. ; Krieger, K. ; Mayer, H. ; Meisl, G. ; Potzel, S. ; Rohde, V. ; Sieglin, B. ; Terra, A. ; Neu, R. ; Linsmeier, Ch. ; Team, EUROfusion MST1. / Surface modification of He pre-exposed tungsten samples by He plasma impact in the divertor manipulator of ASDEX Upgrade. In: Nuclear Materials and Energy. 2017 ; Vol. 12. pp. 575-581.
    @article{390a9f219bc242f495ba5c9a74e8f7af,
    title = "Surface modification of He pre-exposed tungsten samples by He plasma impact in the divertor manipulator of ASDEX Upgrade",
    abstract = "Tungsten (W) will be used as material for plasma-facing components (PFCs) in the divertor of ITER and interact with Helium (He) ions either from initial He plasma operation or from Deuterium-Tritium (DT) fusion reactions in the active operation phase. Laboratory experiments reported that in a specific operational window of impact energy, ion fluence, and surface temperature (E in ≥ 20 eV, ϕ ≥ 1 × 10 24 He+mB t=2.5T,I p=0.8MA,P aux≃8.0MW T surf ≥ 1000 K) a modification of W surfaces occurs resulting in the formation of He-induced W nanostructures. Experiments in ASDEX Upgrade H-mode plasmas (E in=37keV T, ϕ≃0.75×10 24He 0m −2 MA, P aux ≃ 8.0 MW) in He have been carried out to investigate in detail (a) the potential growth of W nanostructures on pre-damaged W samples incorporating He nanobubbles, and (b) the potential ELM-induced erosion of W nanostructure. Both W surface modifications were generated artificially in the GLADIS facility by He bombardment of W samples at ϕ≃1×10 24He 0m −2 keV (a) to ϕ ≃ 0.75 × 10 24 He 0mϕ≃1.6×10 24He +m −2 at T surf ≃ 1800 K and (b) ϕ ≃ 1 × 10 24 He 0m−2 at T surf ≃ 2300 K prior to exposure in the divertor manipulator of ASDEX Upgrade. Though in part (a) conditions of W nanostructure growth with a total He ion fluence of ϕ ≃ 1.6 × 10 24 He+m−2 and peak He ion impact energies above 150 eV were met, no growth could be detected. In part (b) lower density plasmas with more pronounced type I ELMs, carrying energetic He ions in the keV range, were executed with the strike-line positioned on 2 µm thick W nanostructure accumulating a fluence of ϕ ≃ 0.8 × 10 24 He+m−2. Post-mortem analysis revealed that co-deposition by predominantly W, and Boron (B), eroded at the main chamber wall and transported into the divertor, took place on all W samples. Erosion of W nanostructure or its formation was hindered by the fact that the outer divertor at the location of the samples was turned under these He plasma conditions into a net deposition zone by W, B and Carbon (C) ions. The surface morphology with large roughness and effective surface area act as a catcher for the impinging impurities. Thus, apart from operation in the existence diagram of W nanostructure with respect to T surf, ϕ, and E in, also the impinging impurity flux contribution needs to be considered in predictions concerning the formation of W nanostructures.",
    keywords = "PSI, ASDEX Upgrade, ITER, W divertor, W nanostructure, helium",
    author = "S. Brezinsek and A. Hakola and H. Greuner and M. Balden and A. Kallenbach and M. Oberkofler and {De Temmerman}, G. and D. Douai and A. Lahtinen and B. B{\"o}swirth and D. Brida and R. Caniello and D. Carralero and S. Elgeti and K. Krieger and H. Mayer and G. Meisl and S. Potzel and V. Rohde and B. Sieglin and A. Terra and R. Neu and Ch. Linsmeier and Team, {EUROfusion MST1}",
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    day = "1",
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    language = "English",
    volume = "12",
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    Brezinsek, S, Hakola, A, Greuner, H, Balden, M, Kallenbach, A, Oberkofler, M, De Temmerman, G, Douai, D, Lahtinen, A, Böswirth, B, Brida, D, Caniello, R, Carralero, D, Elgeti, S, Krieger, K, Mayer, H, Meisl, G, Potzel, S, Rohde, V, Sieglin, B, Terra, A, Neu, R, Linsmeier, C & Team, EUROMST 2017, 'Surface modification of He pre-exposed tungsten samples by He plasma impact in the divertor manipulator of ASDEX Upgrade', Nuclear Materials and Energy, vol. 12, pp. 575-581. https://doi.org/10.1016/j.nme.2016.11.002

    Surface modification of He pre-exposed tungsten samples by He plasma impact in the divertor manipulator of ASDEX Upgrade. / Brezinsek, S.; Hakola, A.; Greuner, H.; Balden, M.; Kallenbach, A.; Oberkofler, M.; De Temmerman, G.; Douai, D.; Lahtinen, A.; Böswirth, B.; Brida, D.; Caniello, R.; Carralero, D.; Elgeti, S.; Krieger, K.; Mayer, H.; Meisl, G.; Potzel, S.; Rohde, V.; Sieglin, B.; Terra, A.; Neu, R.; Linsmeier, Ch.; Team, EUROfusion MST1.

    In: Nuclear Materials and Energy, Vol. 12, 01.08.2017, p. 575-581.

    Research output: Contribution to journalArticleScientificpeer-review

    TY - JOUR

    T1 - Surface modification of He pre-exposed tungsten samples by He plasma impact in the divertor manipulator of ASDEX Upgrade

    AU - Brezinsek, S.

    AU - Hakola, A.

    AU - Greuner, H.

    AU - Balden, M.

    AU - Kallenbach, A.

    AU - Oberkofler, M.

    AU - De Temmerman, G.

    AU - Douai, D.

    AU - Lahtinen, A.

    AU - Böswirth, B.

    AU - Brida, D.

    AU - Caniello, R.

    AU - Carralero, D.

    AU - Elgeti, S.

    AU - Krieger, K.

    AU - Mayer, H.

    AU - Meisl, G.

    AU - Potzel, S.

    AU - Rohde, V.

    AU - Sieglin, B.

    AU - Terra, A.

    AU - Neu, R.

    AU - Linsmeier, Ch.

    AU - Team, EUROfusion MST1

    PY - 2017/8/1

    Y1 - 2017/8/1

    N2 - Tungsten (W) will be used as material for plasma-facing components (PFCs) in the divertor of ITER and interact with Helium (He) ions either from initial He plasma operation or from Deuterium-Tritium (DT) fusion reactions in the active operation phase. Laboratory experiments reported that in a specific operational window of impact energy, ion fluence, and surface temperature (E in ≥ 20 eV, ϕ ≥ 1 × 10 24 He+mB t=2.5T,I p=0.8MA,P aux≃8.0MW T surf ≥ 1000 K) a modification of W surfaces occurs resulting in the formation of He-induced W nanostructures. Experiments in ASDEX Upgrade H-mode plasmas (E in=37keV T, ϕ≃0.75×10 24He 0m −2 MA, P aux ≃ 8.0 MW) in He have been carried out to investigate in detail (a) the potential growth of W nanostructures on pre-damaged W samples incorporating He nanobubbles, and (b) the potential ELM-induced erosion of W nanostructure. Both W surface modifications were generated artificially in the GLADIS facility by He bombardment of W samples at ϕ≃1×10 24He 0m −2 keV (a) to ϕ ≃ 0.75 × 10 24 He 0mϕ≃1.6×10 24He +m −2 at T surf ≃ 1800 K and (b) ϕ ≃ 1 × 10 24 He 0m−2 at T surf ≃ 2300 K prior to exposure in the divertor manipulator of ASDEX Upgrade. Though in part (a) conditions of W nanostructure growth with a total He ion fluence of ϕ ≃ 1.6 × 10 24 He+m−2 and peak He ion impact energies above 150 eV were met, no growth could be detected. In part (b) lower density plasmas with more pronounced type I ELMs, carrying energetic He ions in the keV range, were executed with the strike-line positioned on 2 µm thick W nanostructure accumulating a fluence of ϕ ≃ 0.8 × 10 24 He+m−2. Post-mortem analysis revealed that co-deposition by predominantly W, and Boron (B), eroded at the main chamber wall and transported into the divertor, took place on all W samples. Erosion of W nanostructure or its formation was hindered by the fact that the outer divertor at the location of the samples was turned under these He plasma conditions into a net deposition zone by W, B and Carbon (C) ions. The surface morphology with large roughness and effective surface area act as a catcher for the impinging impurities. Thus, apart from operation in the existence diagram of W nanostructure with respect to T surf, ϕ, and E in, also the impinging impurity flux contribution needs to be considered in predictions concerning the formation of W nanostructures.

    AB - Tungsten (W) will be used as material for plasma-facing components (PFCs) in the divertor of ITER and interact with Helium (He) ions either from initial He plasma operation or from Deuterium-Tritium (DT) fusion reactions in the active operation phase. Laboratory experiments reported that in a specific operational window of impact energy, ion fluence, and surface temperature (E in ≥ 20 eV, ϕ ≥ 1 × 10 24 He+mB t=2.5T,I p=0.8MA,P aux≃8.0MW T surf ≥ 1000 K) a modification of W surfaces occurs resulting in the formation of He-induced W nanostructures. Experiments in ASDEX Upgrade H-mode plasmas (E in=37keV T, ϕ≃0.75×10 24He 0m −2 MA, P aux ≃ 8.0 MW) in He have been carried out to investigate in detail (a) the potential growth of W nanostructures on pre-damaged W samples incorporating He nanobubbles, and (b) the potential ELM-induced erosion of W nanostructure. Both W surface modifications were generated artificially in the GLADIS facility by He bombardment of W samples at ϕ≃1×10 24He 0m −2 keV (a) to ϕ ≃ 0.75 × 10 24 He 0mϕ≃1.6×10 24He +m −2 at T surf ≃ 1800 K and (b) ϕ ≃ 1 × 10 24 He 0m−2 at T surf ≃ 2300 K prior to exposure in the divertor manipulator of ASDEX Upgrade. Though in part (a) conditions of W nanostructure growth with a total He ion fluence of ϕ ≃ 1.6 × 10 24 He+m−2 and peak He ion impact energies above 150 eV were met, no growth could be detected. In part (b) lower density plasmas with more pronounced type I ELMs, carrying energetic He ions in the keV range, were executed with the strike-line positioned on 2 µm thick W nanostructure accumulating a fluence of ϕ ≃ 0.8 × 10 24 He+m−2. Post-mortem analysis revealed that co-deposition by predominantly W, and Boron (B), eroded at the main chamber wall and transported into the divertor, took place on all W samples. Erosion of W nanostructure or its formation was hindered by the fact that the outer divertor at the location of the samples was turned under these He plasma conditions into a net deposition zone by W, B and Carbon (C) ions. The surface morphology with large roughness and effective surface area act as a catcher for the impinging impurities. Thus, apart from operation in the existence diagram of W nanostructure with respect to T surf, ϕ, and E in, also the impinging impurity flux contribution needs to be considered in predictions concerning the formation of W nanostructures.

    KW - PSI

    KW - ASDEX Upgrade

    KW - ITER

    KW - W divertor

    KW - W nanostructure

    KW - helium

    UR - http://www.scopus.com/inward/record.url?scp=85009233134&partnerID=8YFLogxK

    U2 - 10.1016/j.nme.2016.11.002

    DO - 10.1016/j.nme.2016.11.002

    M3 - Article

    VL - 12

    SP - 575

    EP - 581

    JO - Nuclear Materials and Energy

    JF - Nuclear Materials and Energy

    SN - 2352-1791

    ER -